Name____________________________
1. Nuclear Overhauser Effect, n.o.e., is:
a) the name given to the reason magnetic moment preccess in a magnetic field.
b) the effective coupling between one nuclei and a neighboring nuclei
c) the enhanced intensity one gets in a C-13 spectrum when the H attached to it is decoupled.
d) the effect one gets by giving a nuclei a 180 degree pulse.
2. The maximum NMR signal is obtained by a single pulse of ________ degrees.
a) 45 b) 90 c) 180 d) 360
3. A fast relaxation time (a low
value of T2) will lead to a) narrow
peaks b) broad peaks
c) low intensity peaks d) high
intensity peaks.
4. The signal to noise ratio is
50:1 after 16 transients. What
would the signal to noise ratio be after just one pulse?
a) 4.2:1 b) 200:1 c) 12.5:1 d)
800:1 e) 80:1
5. All other things being equal, by what factor
would you multiply NT in order to get the same signal to
noise ratio on a sample that is
1/10 as concentrated as the
original.
a) .01 b) .1 c) 1 d) 10 e) 100
6. The 90o pulse width for an instrument is 12 microseconds. If the a 24 microsecond pulse is given on the x axis, where will the magnetic vector of the nucleus (initially on the z axis) end up immediately after the pulse?.
a) -z axis b) -x axis c) -y axis d) half way between the x and the y axis. e) +z axis.
Name____________________________
1. Nuclear Overhauser Effect, n.o.e., is:
a) the name given to the reason magnetic moment preccess in
a magnetic field.
b) the effective coupling between one nuclei and a
neighboring nuclei
c) the enhanced intensity one gets in a C-13 spectrum when
the H attached to it is decoupled.
d) the effect one gets by giving a nuclei a 180 degree
pulse.
2. The maximum
NMR signal is obtained by a single pulse of ________ degrees.
a) 45 b) 90 c) 180 d) 360
3. A fast relaxation time (a low
value of T2) will lead to a) narrow
peaks b) broad peaks
c) low intensity peaks d) high
intensity peaks.
4. The signal to noise ratio is
50:1 after 16 transients. What
would the signal to noise ratio be after just one pulse?
a) 4.2:1 b) 200:1 c) 12.5:1 d)
800:1 e) 80:1
5. All other things being equal, by what factor
would you multiply NT in order to get the same signal to
noise ratio on a sample that is
1/10 as concentrated as the
original.
a) .01 b) .1 c) 1 d) 10 e) 100
6. The 90o pulse width for an instrument is 12
microseconds. If the a 24
microsecond pulse is given on the x axis, where will the magnetic vector of the
nucleus (initially on the z axis) end up immediately after the pulse?.
a) -z axis b)
-x axis c) -y axis d) half way between the x and the y axis. e) +z axis.